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Effect of squeeze, homogenization, and freezing treatments on particle diameter and rheological properties of palygorskite
Department环境材料与生态化学研究发展中心
Xu JX(徐继香)1,2; Wang WB(王文波)1; Wang AQ(王爱勤)1; Wang AQ(王爱勤)
2014
Source PublicationAdvanced Powder Technology
ISSN0921-8831
Volume25Issue:3Pages:968-977
AbstractThe natural palygorskite exist as aggregates or bundles via weak electrostatic and van der Waals interactions. A new method for effective disaggregation of bundles was developed via freezing combined with squeeze and homogenization processes. In this work, the effects of squeeze, homogenization, and freezing treatments on particle size and rheological properties of palygorskite were investigated systematically by particle diameter distribution, steady shear, and linear oscillatory measurements. The influences of squeezing times, homogenization pressure, and freezing time on shear stress and shear modulus were studied in detail. The association capacity of rods in the obtained suspensions was discussed according to a power law of the form Y = kyCn. The correlation among the dispersion of palygorskite, the aspect ratio of the rods, and the rheological properties was discussed. The diameter distribution changed from 4.3 to 3.0 mu m of natural palygorskite to 1.8 mu m of sample squeezed for two times, frozen at -18 degrees C for 4 h, and homogenized at 10 MPa. The suspension with higher shear stress and shear modulus was obtained after squeezed for three times and homogenized at 30 MPa.
KeywordPalygorskite Mechanical Treatment Rheological Properties Particle Size
Subject Area环境材料与生态化学
DOI10.1016/j.apt.2014.01.019
Funding Organization“863” Project of the Ministry of Science and Technology, PR China (No. 2013AA032003);the Science and Technology Support Project of Jiangsu Provincial Sci. & Tech. Department (No. BE2012113)
Indexed BySCI
If2.638
Language英语
Funding Project功能复合材料组
compositor第一作者单位
Citation statistics
Cited Times:13[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.licp.cn/handle/362003/6550
Collection环境材料与生态化学研究发展中心
Corresponding AuthorWang AQ(王爱勤)
Affiliation1.Chinese Acad Sci, Lanzhou Inst Chem Phys, R&D Ctr Xuyi Palygorskite Appl Technol, Lanzhou 730000, Peoples R China
2.Qingdao Univ Sci & Technol, Key Lab Ecochem Engn, Minist Educ, Coll Chem & Mol Engn, Qingdao 266042, Peoples R China
Recommended Citation
GB/T 7714
Xu JX,Wang WB,Wang AQ,et al. Effect of squeeze, homogenization, and freezing treatments on particle diameter and rheological properties of palygorskite[J]. Advanced Powder Technology,2014,25(3):968-977.
APA Xu JX,Wang WB,Wang AQ,&王爱勤.(2014).Effect of squeeze, homogenization, and freezing treatments on particle diameter and rheological properties of palygorskite.Advanced Powder Technology,25(3),968-977.
MLA Xu JX,et al."Effect of squeeze, homogenization, and freezing treatments on particle diameter and rheological properties of palygorskite".Advanced Powder Technology 25.3(2014):968-977.
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