Benzimidazole modified silica as a novel reversed-phase and anion-exchange mixed-mode stationary phase for HPLC | |
Department | 中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室 |
Sun, Min1; Feng JJ(冯娟娟)2,3; Luo, Chuannan1; Liu X(刘霞)2; Jiang SX(蒋生祥)2 | |
2013 | |
Source Publication | Talanta |
ISSN | 0039-9140 |
Volume | 105Pages:135-141 |
Abstract | A novel stationary phase based on benzimidazole modified silica was prepared and evaluated as reversed-phase and anion-exchange mixed-mode stationary phase for high performance liquid chromatography (HPLC). Using the phase, polycyclic aromatic hydrocarbons, phthalates, anilines and phenols were respectively separated depending on formation of different types of chemical bonds like hydrogen bonding, π-π stacking, electrostatic forces and hydrophobic interactions by reversed-phase chromatography; inorganic and organic anions were also separated mainly through anion-exchange and pi-pi( interactions by anion-exchange chromatography with high resolution and column efficiency. The proposed benzimidazole modified silica is a promising mixed-mode stationary phase for the separation of complex samples in HPLC. |
Keyword | Benzimidazole Modified Silica Stationary Phase Mixed-mode Reversed-phase Chromatography Anion-exchange Chromatography Hplc |
Subject Area | 分析化学与药物化学 |
DOI | 10.1016/j.talanta.2012.11.077 |
Funding Organization | the National Natural Science Foundation of China (NSFC, no. 21205048);the Shandong Provincial Natural Science Foundation of China (Nos. ZR2012BQ018;ZR2012BM020);the Doctoral Foundation of University of Jinan (No. XBS1207) |
Indexed By | SCI |
If | 3.511 |
Language | 英语 |
Funding Project | 药物分离材料研究组 |
compositor | 第二作者单位 |
Citation statistics | |
Document Type | 期刊论文 |
Identifier | http://ir.licp.cn/handle/362003/18232 |
Collection | 中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室 |
Corresponding Author | Luo, Chuannan |
Affiliation | 1.Univ Jinan, Sch Chem & Chem Engn, Key Lab Chem Sensing & Anal Univ Shandong, Jinan 250022, Peoples R China 2.Chinese Acad Sci, Lanzhou Inst Chem Phys, Key Lab Nat Med Gansu Prov, Key Lab Chem Northwest Plant Resources, Lanzhou 730000, Peoples R China 3.Univ Chinese Acad Sci, Beijing 100039, Peoples R China |
Recommended Citation GB/T 7714 | Sun, Min,Feng JJ,Luo, Chuannan,et al. Benzimidazole modified silica as a novel reversed-phase and anion-exchange mixed-mode stationary phase for HPLC[J]. Talanta,2013,105:135-141. |
APA | Sun, Min,Feng JJ,Luo, Chuannan,Liu X,&Jiang SX.(2013).Benzimidazole modified silica as a novel reversed-phase and anion-exchange mixed-mode stationary phase for HPLC.Talanta,105,135-141. |
MLA | Sun, Min,et al."Benzimidazole modified silica as a novel reversed-phase and anion-exchange mixed-mode stationary phase for HPLC".Talanta 105(2013):135-141. |
Files in This Item: | ||||||
File Name/Size | DocType | Version | Access | License | ||
Talanta 105 (2013) 1(725KB) | 期刊论文 | 作者接受稿 | 开放获取 | CC BY-NC-SA | View Application Full Text |
Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.
Edit Comment