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The preparation of CeF3 nanocluster capped with oleic acid by extraction method and application to lithium grease
Department固体润滑国家重点实验室
Wang LB(王李波); Zhang M(张敏); Wang XB(王晓波); Liu WM(刘维民)
2008
Source PublicationMaterials Research Bulletin
ISSN0025-5408
Volume43Pages:2220-2227
AbstractCeF3 nanocluster surface-capped with oleic acid (coded as OA-CeF3) were prepared using extraction method. The resulting OA-CeF3 nanocluster was characterized by means of transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transformation infrared spectrometry (FTIR), and X-ray photoelectron spectroscopy (XPS). The effect of the OA-CeF3 nanocluster as an additive in synthetic lithiumgreasewas investigated using a four-ball friction and wear tester. It was found that the as-prepared OA-CeF3 nanocluster had a broad size distribution, with the average diameter to be about 20 nm, which was confirmed by both the XRD and TEM analytical results. The oleic acid as the capping agent was chemically bonded to the CeF3 nanocores via strong chemical interaction. The OA-CeF3 nanocluster as the additive led to an obvious improvement in the antiwear and extreme pressure properties of the synthetic lithium grease. However, the OA-CeF3 nanocluster as the additive had little effect on the friction-reducing behavior of the lithium grease
KeywordFluorides Nanostructures Chemical Synthesis X-ray Diffraction Mechanical Properties
Subject Area材料科学与物理化学
Funding Organizationthe National Basic Research Program of China (Grant No. 2007CB607601);the National Natural Science Foundation of China in the name of ‘‘Innovative Group Fund’’ (Grant No. 50421502)
Indexed BySCI
Language英语
Funding Project工业润滑研究组 ; 空间润滑材料组
Citation statistics
Cited Times:61[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.licp.cn/handle/362003/2671
Collection固体润滑国家重点实验室(LSL)
Corresponding AuthorLiu WM(刘维民)
Recommended Citation
GB/T 7714
Wang LB,Zhang M,Wang XB,et al. The preparation of CeF3 nanocluster capped with oleic acid by extraction method and application to lithium grease[J]. Materials Research Bulletin,2008,43:2220-2227.
APA 王李波,张敏,王晓波,&刘维民.(2008).The preparation of CeF3 nanocluster capped with oleic acid by extraction method and application to lithium grease.Materials Research Bulletin,43,2220-2227.
MLA 王李波,et al."The preparation of CeF3 nanocluster capped with oleic acid by extraction method and application to lithium grease".Materials Research Bulletin 43(2008):2220-2227.
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