The preparation of CeF3 nanocluster capped with oleic acid by extraction method and application to lithium grease | |
Department | 固体润滑国家重点实验室 |
Wang LB(王李波); Zhang M(张敏); Wang XB(王晓波); Liu WM(刘维民) | |
2008 | |
Source Publication | Materials Research Bulletin |
ISSN | 0025-5408 |
Volume | 43Pages:2220-2227 |
Abstract | CeF3 nanocluster surface-capped with oleic acid (coded as OA-CeF3) were prepared using extraction method. The resulting OA-CeF3 nanocluster was characterized by means of transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transformation infrared spectrometry (FTIR), and X-ray photoelectron spectroscopy (XPS). The effect of the OA-CeF3 nanocluster as an additive in synthetic lithiumgreasewas investigated using a four-ball friction and wear tester. It was found that the as-prepared OA-CeF3 nanocluster had a broad size distribution, with the average diameter to be about 20 nm, which was confirmed by both the XRD and TEM analytical results. The oleic acid as the capping agent was chemically bonded to the CeF3 nanocores via strong chemical interaction. The OA-CeF3 nanocluster as the additive led to an obvious improvement in the antiwear and extreme pressure properties of the synthetic lithium grease. However, the OA-CeF3 nanocluster as the additive had little effect on the friction-reducing behavior of the lithium grease |
Keyword | Fluorides Nanostructures Chemical Synthesis X-ray Diffraction Mechanical Properties |
Subject Area | 材料科学与物理化学 |
Funding Organization | the National Basic Research Program of China (Grant No. 2007CB607601);the National Natural Science Foundation of China in the name of ‘‘Innovative Group Fund’’ (Grant No. 50421502) |
Indexed By | SCI |
Language | 英语 |
Funding Project | 工业润滑研究组 ; 空间润滑材料组 |
Citation statistics | |
Document Type | 期刊论文 |
Identifier | http://ir.licp.cn/handle/362003/2671 |
Collection | 固体润滑国家重点实验室(LSL) |
Corresponding Author | Liu WM(刘维民) |
Recommended Citation GB/T 7714 | Wang LB,Zhang M,Wang XB,et al. The preparation of CeF3 nanocluster capped with oleic acid by extraction method and application to lithium grease[J]. Materials Research Bulletin,2008,43:2220-2227. |
APA | 王李波,张敏,王晓波,&刘维民.(2008).The preparation of CeF3 nanocluster capped with oleic acid by extraction method and application to lithium grease.Materials Research Bulletin,43,2220-2227. |
MLA | 王李波,et al."The preparation of CeF3 nanocluster capped with oleic acid by extraction method and application to lithium grease".Materials Research Bulletin 43(2008):2220-2227. |
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