| Simplified hydrothermal synthesis and optical properties of core-shell ZnS microspheres | |
| Department | 固体润滑国家重点实验室 |
Li, Maohua1,2; Lu, Yi1,2; Hao JY(郝俊英)3 ; Long, Zerong2; Yang, Bo2; Liu, Yumei1; Hao JY(郝俊英)
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| 2014 | |
| Source Publication | OPTOELECTRONICS AND ADVANCED MATERIALS-RAPID COMMUNICATIONS
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| ISSN | 1842-6573 |
| Volume | 8Issue:11-12Pages:1091-1095 |
| Abstract | Zinc acetylacetonate and thiourea are reacted in a 30:10 mixed water: glycerin solvent for 12 hours at 130 C to synthesize "core-shell" ZnS microspheres. The ZnS microspheres are characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), x-ray diffraction (XRD), x-ray photoelectron spectroscopy (XPS), energy dispersive x-ray (EDX), high-resolution transmission electron microscopy (HRTEM); and selected area electron diffraction (SEAD). Ultraviolet-visible spectra (UV-vis) and photoluminescence spectroscopy (PL) were used in an optical study of the product. The results show that the synthesized ZnS microspheres have a diameter of 3-5 micrometers, a smooth shell surface, and an inner core structure. The existence of glycerin is crucial to the formation of spherical ZnS. no spherical particles are obtained in reaction systems without glycerin, and a decrease in glycerin content of the system reduces the yield of spherical products. |
| Keyword | Hydrothermal Reaction Core-shell Structure Zns Glycerin |
| Funding Organization | the National Natural Science Foundation of China (No. 51375471);the major project of Xinjiang Bureau of Quality and Technical Supervision (No. 2013-01);the Acience and Technology Project of State Quality Inspection Administration (2013QK086) |
| Indexed By | SCI |
| If | 0.394 |
| Language | 英语 |
| Funding Project | 空间润滑材料组 |
| compositor | 第三作者单位 |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.licp.cn/handle/362003/20709 |
| Collection | 固体润滑国家重点实验室（LSL） |
| Corresponding Author | Liu, Yumei; Hao JY(郝俊英) |
| Affiliation | 1.Xinjiang Univ, Coll Chem & Chem Engn, Urumqi Xinjing 830046, Peoples R China 2.Xinjiang Supervis & Inspect Inst Prod Qual, Urumqi Xinjing 830011, Peoples R China 3.Chinese Acad Sci, Lanzhou Inst Chem Phys, State key Lab Solid Lubricat, Lanzhou 730000, Peoples R China |
| Recommended Citation GB/T 7714 | Li, Maohua,Lu, Yi,Hao JY,et al. Simplified hydrothermal synthesis and optical properties of core-shell ZnS microspheres[J]. OPTOELECTRONICS AND ADVANCED MATERIALS-RAPID COMMUNICATIONS,2014,8(11-12):1091-1095. |
| APA | Li, Maohua.,Lu, Yi.,Hao JY.,Long, Zerong.,Yang, Bo.,...&郝俊英.(2014).Simplified hydrothermal synthesis and optical properties of core-shell ZnS microspheres.OPTOELECTRONICS AND ADVANCED MATERIALS-RAPID COMMUNICATIONS,8(11-12),1091-1095. |
| MLA | Li, Maohua,et al."Simplified hydrothermal synthesis and optical properties of core-shell ZnS microspheres".OPTOELECTRONICS AND ADVANCED MATERIALS-RAPID COMMUNICATIONS 8.11-12(2014):1091-1095. |
| Files in This Item: | ||||||
| File Name/Size | DocType | Version | Access | License | ||
| LZ01029283.pdf（498KB） | 期刊论文 | 作者接受稿 | 开放获取 | CC BY-NC-SA | View Application Full Text | |
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