直流法制备类富勒烯碳氢薄膜的摩擦学性能研究
Department先进润滑与防护材料研究发展中心
欧玉静1; 郭俊猛1,2; 王永富2; 高凯雄2; 梁爱民2; 张斌2; 张俊彦2
The second department固体润滑国家重点实验室
2015
Source Publication摩擦学学报
ISSN1004-0595
Volume35Issue:1Pages:82-89
Abstract

Hydrogenated fullerene-like carbon (FL-C∶H) films were deposited on Si (100) substrates by a direct current plasma enhanced chemical vapor deposition(dc-PECVD) technique using pure CH4 as feedstock. Simplify the hydrogen fullerene (FL-C: H) films prepared by pulsed bias - assisted plasma chemical vapor process (mc-PECVD). The microstructures and the FL content of the FL-C∶ H films were characterized by high transmission electron microscopy and Raman spectrum. The mechanical properties and friction behaviors of the films were investigated by using a Nano-indenter and a ball- on-disk tester. Results show that compared with the hydrogen-containing fullerene -like filmsprepared by pulse bias-assisted method, FL-C∶ H films prepared by dc method that exhibited a similar icrostructure, superior excellent mechanical properties and tribological performance, and these films showed low sensitivity to load , frequency and relative humidity.

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采用直流等离子体化学气相沉积(dc-PECVD) 技术,以甲烷为前驱体,在单晶硅表面制备了含氢类富勒烯(FL-C∶H) 薄膜. 简化了含氢类富勒烯(FL-C∶ H) 薄膜的脉冲偏压协助等离子体化学气相制备过程(mc-PECVD),通过高分辨率透射电镜和拉曼光谱确定了FL-C∶H 薄膜的微观结构和薄膜内的富勒烯含量; 通过纳米压痕和往复摩擦试验对比了两种方法制备的FL-C∶H 与传统的DLC 薄膜的硬度及摩擦性能.结果表明: 与用脉冲偏压协助方案制备的含氢类富勒烯薄膜相比,直流方案制备的FL-C∶H薄膜具有相似的微观结构,更优异的机械特性及摩擦学性能,同时该薄膜表现出对载荷、频率和相对湿度的低敏感性.

Keyword直流 类富勒烯 脉冲偏压协助 低敏感性 Direct Current Fullerene-like Pulse Bias-assisted Low Sensitivity
Subject Area材料科学与物理化学
DOI10.16078 /j.tribology.2015.01.012
Funding Organization国家973 项目(2013CB632304);国家自然科学基金(51275508;51205383)
Indexed ByEI&CSCD
If0.6263(CSCD-JCR)
Language中文
Funding Project纳米润滑研究组
compositor第二作者单位
Citation statistics
Document Type期刊论文
Identifierhttp://ir.licp.cn/handle/362003/19137
Collection中国科学院材料磨损与防护重点实验室/先进润滑与防护材料研究发展中心
固体润滑国家重点实验室(LSL)
Corresponding Author张俊彦
Affiliation1.兰州理工大学
2.中国科学院兰州化学物理研究所
Corresponding Author AffilicationLanzhou Institute of Chemical Physics,Chinese Academy of Sciences
Recommended Citation
GB/T 7714
欧玉静,郭俊猛,王永富,等. 直流法制备类富勒烯碳氢薄膜的摩擦学性能研究[J]. 摩擦学学报,2015,35(1):82-89.
APA 欧玉静.,郭俊猛.,王永富.,高凯雄.,梁爱民.,...&张俊彦.(2015).直流法制备类富勒烯碳氢薄膜的摩擦学性能研究.摩擦学学报,35(1),82-89.
MLA 欧玉静,et al."直流法制备类富勒烯碳氢薄膜的摩擦学性能研究".摩擦学学报 35.1(2015):82-89.
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